Polarographic Determination of Carbonyl Groups in Starches by Using o-Phenylenediamine
نویسندگان
چکیده
منابع مشابه
Determination of Selenium(IV) Using o-Phenylenediamine by Differential Pulse Polarography/Interference of Metal Ions
Determination of selenium in biological and environmental samples is usually difficult due to its trace or ultra-trace quantities, pre-concentration stages, destruction of organic matrices by acid digestion and oxygen plasma combustion followed by separation from interfering metal ions such as ion exchange separation, solvent extraction or hydride generation. Selective separation of selenium is...
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چکیده هدف از این کار بررسی الکترواکسیداسیون کتکول و مشتقات آن در حضور 4-فنیل سمی کاربامازید بوده است اکسیداسیون کتکولها ترکیبات نا پایدار کینونها را تولید می کنند که این ترکیبات می تواند در واکنش مایکل بعنوان پذیرنده نوکلئوفیل عمل نمایند. در ادامه اکسایش کتکولهای (a-c1) را درحضور 4-فنیل سمی کاربامازید در محلول آب/استونیتریل (90/10)بوسیله ولتامتری چرخه ای و کولن متری در پتانسیل ثابت مورد بررسی ...
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A method is described for determining carbonyl groups that is especially suitable for use with proteins and peptides. It involves the determination of the extinction at 370nm of a sample solution after adding 2,4-dinitrophenylhydrazine. The reaction of 2,4-dinitrophenylhydrazine with pyruvoylglycine and with transaminated ribonuclease T(1) is presented; the isolation of protein hydrazones is di...
متن کاملThe polarographic determination of selenium in urine.
Polarographicdata are presented for the reduction of selenite ion in 3M sulfuric acid, 1M potassium chloride, and 1M ammonia-ammonium chloride. In these first two media two waves are obtained correspondingto the diffusion-controlled reduction of selenite ion to selenium amalgam and the adsorption of selenite ion on the mercury drop, respectively. One wave is obtained in ammonia-ammonium chlorid...
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ژورنال
عنوان ژورنال: Review of Polarography
سال: 1969
ISSN: 0034-6691,1884-7692
DOI: 10.5189/revpolarography.16.43